Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Isethionic Acid | HCID 7866 | — |
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Product | HCID 21932458 | HCID 21932458 | 100% |
Reaction Conditions
| Temperature | 200 fahrenheit |
|---|
Reaction Steps
In a preferred embodiment, diethanol amine is charged to the reaction vessel in a substantially equal molar quantity to a 54 percent aqueous solution the sodium salt of isethionic acid. The reactants then are heated to a temperature of about 200° F. at ambient temperature for a sufficient period of time to separate about 38 percent by weight of the reactants as water in the cold finger trap. The bis-hydroxyethylaminoethane sulfonic acid which is produced in about a 100 percent yield is diluted to about a 50 percent solution by the addition of water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04563291 |
|---|
| Source dataset | uspto-grants-1986_01 |
|---|
| ORD ID | ord-eeb9b39535e04a8f906557b118787816 |
|---|
| Source note | uspto-grants-1986_01 |
|---|