Benzene, 2-chloro-1-(3,4-dinitrophenoxy)-4-(trifluoromethyl)- → methyl P-ethyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinate

Participants

Role	Name	HCID	Charge
Reactant	Benzene, 2-chloro-1-(3,4-dinitrophenoxy)-4-(trifluoromethyl)-	HCID 156238	—
Reactant	Dimethyl ethylphosphonite	HCID 2784207	—
Solvent	Acetonitrile	HCID 6342	—
Product	methyl P-ethyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinate	HCID 13456449	—

Reaction Steps

Following the procedure of Example 1, 1.5 g (4.14 mmol) of 4-(2-chloro-4-trifluoromethylphenoxy)-1,2-dinitrobenzene, 0.81 g (6.6 mmol) of dimethyl ethylphosphonite and 3 ml of acetonitrile are reacted together to give methyl P-ethyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinate.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US04563310
Source dataset	uspto-grants-1986_01
ORD ID	ord-fc423709d0a34091a46373afeb841782
Source note	uspto-grants-1986_01