HuagongsheHuagongshe Chemistry Print Report · For research reference only
methyl P-ethyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinate → P-ethyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | methyl P-ethyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinate | HCID 13456449 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | P-ethyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinic acid | HCID 15589803 | — |
Reaction Steps
Following the method of Example 13, 1 g of methyl P-ethyl-2-nitro-5-(2-chloro-4-trifluoromethyl-phenoxy)phenylphosphinate is reacted with 20 ml of 6N HCl to yield P-ethyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenylphosphinic acid, m.p.=99°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04563310 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-97caebcef83a40f2b33611c26758d3a4 |
| Source note | uspto-grants-1986_01 |