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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1284697Generated: October 30, 2026

1-Bromohexane → Ethyl 2-[(hexyloxy)imino]-3-oxobutanoate

https://huagongshe.com/reaction/1284697

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-BromohexaneHCID 8101—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 178472877HCID 178472877—
SolventDimethylformamideHCID 6228—
ProductEthyl 2-[(hexyloxy)imino]-3-oxobutanoateHCID 53879425—

Reaction Steps

Ethyl 2-hydroxyimino-3-oxobutyrate (syn isomer, 40 g.), N,N-dimethylformamide (200 ml.), potassium carbonate (52 g.) and n-hexyl bromide (41.4 g.) were treated in a similar manner to that of Example F-(1) to give ethyl 2-n-hexyloxyimino-3-oxobutyrate (syn isomer, 60.7 g. oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04563522
Source datasetuspto-grants-1986_01
ORD IDord-c9cb8f4778e04187b52c481f477e7b14
Source noteuspto-grants-1986_01