HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopentane → Ethyl 3-oxo-2-[(pentyloxy)imino]butanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopentane | HCID 8057 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178472877 | HCID 178472877 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Ethyl 3-oxo-2-[(pentyloxy)imino]butanoate | HCID 53697317 | 99.9% |
Reaction Steps
Ethyl 2-hydroxyimino-3-oxobutyrate (syn isomer, 40 g.), N,N-dimethylformamide (200 ml.), potassium carbonate (52 g.) and pentyl bromide (37.9 g.) were treated in a similar manner to that of Example F-(1) to give ethyl 2-pentyloxyimino-3-oxobutyrate (syn isomer, 57.5 g.), oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04563522 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-4cdb7af8fc40492a917287a0cc1245ce |
| Source note | uspto-grants-1986_01 |