HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 54180953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | Sodium Acetate Trihydrate | HCID 23665404 | — |
| Reactant | HCID 54423660 | HCID 54423660 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54180953 | HCID 54180953 | 35.8% |
Reaction Steps
Ethyl 2-n-octyloxyimino-4-chloro-3-oxobutyrate (syn isomer, 169.6 g.), thiourea (42.3 g.), sodium acetate trihydrate (75.5 g.), water (420 ml.) and ethanol (1020 ml.) were treated in a similar manner to that of Example F-(3) to give ethyl 2-(2-aminothiazol-4-yl)-2-n-octyloxyiminoacetate (syn isomer, 65 g.), mp. 77° to 78° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04563522 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-c2aa21ba1595404e861a238b7504a778 |
| Source note | uspto-grants-1986_01 |