HuagongsheHuagongshe Chemistry Print Report · For research reference only
Styrene → HCID 141711, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | 4-Bromobenzaldehyde | HCID 70741 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 141711 | HCID 141711 | 72% |
Reaction Steps
The procedure described in Example 26 is repeated, but using 4.63 g (25 mmols) of 4-bromobenzaldehyde and 3.16 ml (27.5 mmols) of styrene. After a reaction time of 4 hours at 130° C., 3.74 g (18.0 mmols) of 4-formylstilbene are obtained, corresponding to a yield of 72% of theory (conversion figure 7200; Pd content 0.01 mol %).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04564479 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-0e0ef38b663e4ff8bf8779dcb4e3d1cc |
| Source note | uspto-grants-1986_01 |