HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → trans-4'-Propyl-(1,1'-bicyclohexyl)-4-carboxylic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | [1,1'-Bicyclohexyl]-4-carbonitrile, 4'-propyl-, (trans,trans)- | HCID 103365 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | trans-4'-Propyl-(1,1'-bicyclohexyl)-4-carboxylic Acid | HCID 793726 | — |
Reaction Steps
On the other hand, 50 g of 4-propyl-4'-cyanobicyclohexane was dissolved in 50 ml of C2H5OH, and 25 g of KOH and 15 ml of water was added to the resulting solution, after which the resulting mixture was refluxed for 8 hours and poured into dilute hydrochloric acid, and then the acidic solution was extracted with (C2H5)2O and the (C2H5)2O was distilled off. The residue was recrystallized from benzene to obtain 4-propyl-4'-bicyclohexanecarboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04564694 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-1d3e612ccaa24839b4e5754759d4f6d5 |
| Source note | uspto-grants-1986_01 |