Carbon Dioxide → HCID 13282769, compound

HRID 1285105Notes

Reaction equation

HRID 1285105 reaction equation
[CH2:1]1[O:3][CH2:2]1.C(=O)=O.[CH2:7]([NH:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1>CO>[CH2:7]([N:14]([CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH2:2][CH2:1][OH:3])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

Participants

5

Reactant 3

HCID 280Carbon DioxideHCID 6354Ethylene OxideHCID 88404N-Octadecylbenzenemethanamine

Product 1

HCID 13282769HCID 13282769, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

40 ml of ethylene oxide cooled with dry ice are added dropwise into a mixture of 65.9 g of N-benzyl-octadecyl amine and 200 ml of methanol at room temperature within 2 hours; the mixture is stirred for further 3 hours, the solvent removed and the residue purified by column chromatography (silica gel//chloroform).

Workup

  1. customthe solvent removed
  2. customthe residue purified by column chromatography (silica gel//chloroform)

Sources & evidence

ORD record
ord-3463569c6ab34e3db420f72e1645dd3a
Source dataset
uspto-grants-1986_01
Patent number
US04565659

Reaction notes

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