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HRID1285163

反应详情

EQUATION

反应方程式

HRID 1285163 的结构方程式

REACTANTS

反应物

3
结构：CC(C)O
HCID3776

Isopropanol

C3H8O

结构：Cc1nc(CCl)no1
HCID302157

3-(chloromethyl)-5-methyl-1,2,4-oxadiazole

C4H5ClN2O

结构：Cn1c(=O)c2[nH]cnc2n(C)c1=O.[Na]
HCID66973603

未命名化合物

PRODUCTS

生成物

1
结构：CCn1c(=O)c2c(ncn2-c2noc(C)n2)n(C)c1=O
HCID20249897

未命名化合物

收率 74.2%

PROCEDURE

实验过程

20.2 g. of theophylline-sodium, 300 cm3 isopropyl alcohol and 13.2 g. of 3-chloromethyl-5-methyl-1,2,4-oxadiazole are heated under stirring for 10 hours. After processing 20.5 g. (74.2% yield) of 7-(5-methyl-1,2,4-oxadiazol-3-yl)-methyl-theophylline are obtained. M.p.: 134°-135° C.