HCID 19374391, compound → HCID 15283255, compound

HRID 128529Notes

Reaction equation

HRID 128529 reaction equation
C(O[C:6]([NH:8][CH2:9][CH:10]1[CH:18]=[CH:17][CH2:16][CH:15]2[CH:11]1[C:12](=O)[NH:13][C:14]2=O)=O)(C)(C)C.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH3:6][NH:8][CH2:9][CH:10]1[CH:18]=[CH:17][CH2:16][CH:15]2[CH:11]1[CH2:12][NH:13][CH2:14]2

Participants

3

Reactant 2

HCID 19374391HCID 19374391, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 15283255HCID 15283255, compound

Procedure

4-tert.-Butyloxycarbonylaminomethyl-1,3-dioxo-1,3,3a,4,7,7a-hexahydroisoindole is reduced with lithium aluminium hydride by a method analogous to that described in Example A, method IIb: yellow oil.

Sources & evidence

ORD record
ord-329a38c764d1491db22fc3c5e1eb50d4
Source dataset
uspto-grants-1995_11
Patent number
US05464796

Reaction notes

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