HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → Ethoxy(6-phthalimidohexyl)phosphinyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | 2-(6-diethoxyphosphorylhexyl)isoindole-1,3-dione | HCID 256580 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Ethoxy(6-phthalimidohexyl)phosphinyl chloride | HCID 256577 | — |
Reaction Steps
A mixture of (6-phthalimidohexyl)phosphonic acid, diethyl ester, benzene, and phosphorus pentachloride is refluxed according to the procedure of Example 1(f) to give ethoxy(6-phthalimidohexyl)phosphinyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04567167 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-f1aacd43516f4c349bdb402cb078a687 |
| Source note | uspto-grants-1986_01 |