HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → 3-Methylcyclopentyl 4-methylbenzene-1-sulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | 3-Methylcyclopentan-1-ol | HCID 86785 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 3-Methylcyclopentyl 4-methylbenzene-1-sulfonate | HCID 19042338 | 92.5% |
Reaction Steps
3-Methylcyclopentanol (5.0 g, 49.9 mmol) was reacted with p-toluenesulfonyl chloride in pyridine (50 ml) in the same procedure as in Reference Example 7 to obtain 3-methylcyclopentyl p-toluenesulfonate (11.7 g, 46.2 mmol, 92.5% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05464811 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-1c2bbb9f0d6e48939eb0e78124fbb5c0 |
| Source note | uspto-grants-1995_11 |