HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol, 2-fluoro-2,2-dinitro- → 1-Fluoro-1,1,5-trinitro-3-oxa-5azahexane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol, 2-fluoro-2,2-dinitro- | HCID 28189 | — |
| Reactant | Acetic acid, trifluoro-, (methylnitroamino)methyl ester | HCID 13352131 | — |
| Product | 1-Fluoro-1,1,5-trinitro-3-oxa-5azahexane | HCID 13352133 | — |
Reaction Steps
reacting one mole of 2-nitro-2-azapropyl trifluoroacetate with one mole of 2-fluoro-2,2-dinitroethanol in a polar solvent at a temperature of from 0° C. to 40° C. to form 1-fluoro-1,1,5-trinitro-3-oxa-5azahexane, wherein the reaction is run under vacuum to remove trifluoroacetic acid generated by the reaction; and
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04567296 |
| Source dataset | uspto-grants-1986_01 |
| ORD ID | ord-45804309d9454f8fb4d6d054f98606be |
| Source note | uspto-grants-1986_01 |