Hydrazine → 2-(2-Thienylmethoxy)acetic acid, hydrazide

HRID 128656Notes

Reaction equation

HRID 128656 reaction equation
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][O:7][CH2:8][C:9]([O:11]C)=O.[NH2:13][NH2:14]>>[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][O:7][CH2:8][C:9]([NH:13][NH2:14])=[O:11]

Participants

3

Reactant 2

HCID 9321HydrazineHCID 23369384Methyl 2-(2-thienylmethoxy)acetate

Product 1

HCID 217447822-(2-Thienylmethoxy)acetic acid, hydrazide

Procedure

2-(2-thienylmethoxy)acetic acid, hydrazide (20) was prepared from methyl 2-(2-thienylmethoxy)acetate (19) (3.6 mmol), prepared in the manner described above in Example 19, and hydrazine (3.6 mmol) in the manner described above in Example 12 to yield 0.60 g (90%) of product.

Workup

  1. customprepared in the manner

Sources & evidence

ORD record
ord-cbade2300cab46db901861c8bc257f52
Source dataset
uspto-grants-1995_11
Patent number
US05464830

Reaction notes

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