Benzoyl chloride → HCID 19374853, compound

HRID 128689Notes

Reaction equation

HRID 128689 reaction equation
[S-:1][C:2]#[N:3].[NH4+].[C:5](Cl)(=[O:12])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1.[Cl:14][C:15]1[CH:16]=[N:17][CH:18]=[CH:19][C:20]=1[CH:21]([NH:23][CH2:24][CH2:25][CH3:26])[CH3:22]>>[C:5]([NH:3][C:2](=[S:1])[N:23]([CH:21]([C:20]1[CH:19]=[CH:18][N:17]=[CH:16][C:15]=1[Cl:14])[CH3:22])[CH2:24][CH2:25][CH3:26])(=[O:12])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

Participants

4

Reactant 3

HCID 7412Benzoyl chlorideHCID 15666Ammonium thiocyanateHCID 19374909HCID 19374909, compound2×

Product 1

HCID 19374853HCID 19374853, compound

Procedure

Prepare this compound according to the process described in Step A of Preparation XV, from 1.14 g of ammonium thiocyanate, 1.74 ml of benzoyl chloride and 2.7 g of N-[1-(3-chloro-4-pyridyl)ethyl]propylamine (Compound 22).

Workup

  1. customPrepare this compound

Sources & evidence

ORD record
ord-b56177e2740147488c5f2a4994f342c3
Source dataset
uspto-grants-1995_11
Patent number
US05464847

Reaction notes

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