HRID1287182

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：[N-]=[N+]=C1C=C(S(=O)(=O)Cl)c2ccccc2C1=O

HCID136654451

1-Naphthalenesulfonyl chloride, 3-diazo-3,4-dihydro-4-oxo-

C10H5ClN2O3S

结构：[N-]=[N+]=Nc1ccc(OS(=O)(=O)c2cccc3c2C=CC(=[N+]=[N-])C3=O)cc1

HCID178514500

未命名化合物

PRODUCTS

生成物

结构：[N-]=[N+]=Nc1ccc(OS(=O)(=O)C2=CC(=[N+]=[N-])C(=O)c3ccccc32)cc1

HCID178514501

未命名化合物

PROCEDURE

实验过程

This compound is prepared in a similar manner to Compound 1 but 2-diazo-1,2-dihydro-1-oxonaphthalene-4-sulfonyl chloride (2.2 grams) is used instead of the corresponding 5-sulfonyl chloride. The product is crystallized from ethanol. Yield of Compound 7 as a pure product is 1.1 gram, m.p. 131°-132°C (with decomposition).

WORKUP

后处理

customThe product is crystallized from ethanol