Acrylonitrile → Propanenitrile, 3-(hexylthio)-

HRID 1287192Notes

Reaction equation

[CH2:1]([SH:7])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[C:8](#[N:11])[CH:9]=[CH2:10].C[O-].[Na+]>>[CH2:1]([S:7][CH2:10][CH2:9][C:8]#[N:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

Participants

Reactant 3

HCID 7855Acrylonitrile

HCID 81061-Hexanethiol

HCID 10942334Sodium Methoxide

Product 1

HCID 11615258Propanenitrile, 3-(hexylthio)-

Procedure

β-n-Hexylmercaptopropionitrile was prepared according to the procedure of Example 1 using 1-hexanethiol (25.0 g; 0.21 moles), acrylonitrile (11.2 g; 0.21 moles) and sodium methoxide (0.5 g).

Sources & evidence

ORD record: ord-92dcd25575134249b8223032d8a12631
Source dataset: uspto-grants-1976_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03984336

Reaction notes

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