HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylonitrile → 3,3'-(Butane-1,4-diyldisulfanediyl)dipropanenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | Benzyltrimethylammonium hydroxide | HCID 66854 | — |
| Reactant | 1,4-Butanedithiol | HCID 79148 | — |
| Product | 3,3'-(Butane-1,4-diyldisulfanediyl)dipropanenitrile | HCID 21507224 | — |
Reaction Steps
4,9-Dithiadodecanedinitrile was prepared according to the procedure of Example 1 using 1,4-butanedithiol (20.0 g; 0.16 moles), acrylonitrile (17.0 g; 0.32 moles) and benzyltrimethylammonium hydroxide (40% in methanol; 1 ml) as the catalyst.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984336 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-ebfc0ec332534ab8a406278d927751e3 |
| Source note | uspto-grants-1976_10 |