HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Mercaptoethanol → 3-{[2-(2-Cyanoethoxy)ethyl]sulfanyl}propanenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Mercaptoethanol | HCID 1567 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | Benzyltrimethylammonium hydroxide | HCID 66854 | — |
| Product | 3-{[2-(2-Cyanoethoxy)ethyl]sulfanyl}propanenitrile | HCID 220035 | — |
Reaction Steps
4-Oxa-7-thiadecanedinitrile was prepared according to the procedure of Example 1 using 2-mercaptoethanol (25.0 g; 0.32 moles), acrylonitrile (34.0 g; 0.64 moles) and benzyltrimethylammonium hydroxide (40% in methanol; 1 ml) as the catalyst.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984336 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-a8b355b3865f4037948200fd35e91e53 |
| Source note | uspto-grants-1976_10 |