Benzyl mercaptan → 3-(benzylsulfanyl)propanenitrile

HRID 1287199Notes

Reaction equation

HRID 1287199 reaction equation
[C:1]1([CH2:7][SH:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:9](#[N:12])[CH:10]=[CH2:11].C[O-].[Na+]>>[CH2:7]([S:8][CH2:11][CH2:10][C:9]#[N:12])[C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 3

HCID 7509Benzyl mercaptanHCID 7855AcrylonitrileHCID 10942334Sodium Methoxide

Product 1

HCID 2200273-(benzylsulfanyl)propanenitrile

Procedure

β-Benzylmercaptopropionitrile was prepared according to the procedure of Example 1 using α-toluenethiol (25.0 g; 0.20 moles), acrylonitrile (10.6 g; 0.20 moles) and sodium methoxide (0.5 g).

Sources & evidence

ORD record
ord-ebf50ceefd354e97a13c084b41c8637a
Source dataset
uspto-grants-1976_10
Patent number
US03984336

Reaction notes

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