HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 178514930, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 21507660 | HCID 21507660 | — |
| Product | HCID 178514930 | HCID 178514930 | 70.4% |
Reaction Steps
The above nitrile (1 g) was treated with sodium azide (0.66 g) and ammonium chloride (0.57 g) as in the preceding example to give 1-[7(1H-tetrazol-5-yl)-anthraquinon-2-yl] piperidine (0.8 g), m.p. 297-8°C, after crystallisation from dimethylformamide/acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984429 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-77e5c231651847fdba279ba82481a67c |
| Source note | uspto-grants-1976_10 |