HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiazolidinedione → 5-[(4-Hydroxy-3,5-dimethoxyphenyl)methylene]-2,4-thiazolidinedione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiazolidinedione | HCID 5437 | — |
| Reactant | Syringaldehyde | HCID 8655 | — |
| Product | 5-[(4-Hydroxy-3,5-dimethoxyphenyl)methylene]-2,4-thiazolidinedione | HCID 2857669 | 24.2% |
Reaction Steps
Prepared according to the procedure described in Example 1 using 3,5-dimethoxy-4-hydroxybenzaldehyde (4.8 g, 26 mmoles) and 2,4-thiazolidinedione (2.9 g, 25 mmoles). Recrystallization from methanol gave the pure product (1.7 g), mp 248°-249° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05464856 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-a892ed665b4d436cadf84afa0cd0ca53 |
| Source note | uspto-grants-1995_11 |