HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycidol → 3-octadecylsulfanylpropane-1,2-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycidol | HCID 11164 | — |
| Reactant | 1-Octadecanethiol | HCID 17905 | — |
| Product | 3-octadecylsulfanylpropane-1,2-diol | HCID 245962 | — |
Reaction Steps
The octadecyl mercaptan is then condensed with 4 moles glycidol per mole octadecyl mercaptan, first introducing a first molar equivalent of glycidol to obtain 3-octadecylthio-propane-1,2 diol at 80° C, the rest of the glycidol being introduced at 155° C in the course of 2 hours 20 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984480 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-cf331a15f2b34f0bad518a6f66299405 |
| Source note | uspto-grants-1976_10 |