HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenyl Isocyanate → 1-(4-Chlorophenyl)-3-heptanimidoylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenyl Isocyanate | HCID 7693 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Heptanimidamide hydrochloride | HCID 14144282 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1-(4-Chlorophenyl)-3-heptanimidoylurea | HCID 152746821 | — |
Reaction Steps
Following a procedure similar to that described in Example 1 but using 3.9 g. sodium in 300 ml. dry acetone, 24.6 g. heptanamidine hydrochloride, and 23 g. 4-chlorophenyl isocyanate in 100 ml. dry acetone, there was obtained after recrystallization from acetonitrile 29.8 g. of the hydrochloride of 1-(4-chlorophenyl)-3-(heptanimidoyl)urea; m.p. 168°-169°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-0efe26383c3f42d29e20a0127aa8ee84 |
| Source note | uspto-grants-1976_10 |