HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 178444900, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 4-Chlorophenyl isothiocyanate | HCID 16480 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Hexanimidamide hydrochloride | HCID 21420651 | — |
| Solvent | Benzene n-pentane | HCID 19707280 | — |
| Product | HCID 178444900 | HCID 178444900 | — |
Reaction Steps
Following a procedure similar to that described in Example 42 but using 3.4 g. sodium in 300 ml. dry acetone, 22.5 g. hexanamidine hydrochloride, and 25.9 g. 4-chlorophenyl isothiocyanate in 150 ml. dry acetone there was obtained 1-(4-chlorophenyl)-3-(hexanimidoyl)-2-thiourea, m.p. 100°-102°C. (from benzene-n-pentane); hydrochloride (21 g.), m.p. 175°C. (from acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984467 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-d0b562d3dc394efbbaac05d629a649b3 |
| Source note | uspto-grants-1976_10 |