HCID 178444025, compound → HCID 178444023, compound
Reaction equation
Cl.[N+](C1C=CC(NC(NC(=N)CCCC)=O)=CC=1)([O-])=O.Cl.[N+:22]([C:25]1[CH:30]=[CH:29][C:28]([NH:31][C:32]([NH:34][C:35](=[NH:42])[CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH3:41])=[S:33])=[CH:27][CH:26]=1)([O-])=O>>[NH2:22][C:25]1[CH:30]=[CH:29][C:28]([NH:31][C:32]([NH:34][C:35](=[NH:42])[CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH3:41])=[S:33])=[CH:27][CH:26]=1Participants
3
Procedure
By following a procedure similar to that described in Example 10 but substituting for 1-(4-nitrophenyl)-3-(pentanimidoyl)urea hydrochloride an equivalent amount of 1-(4-nitrophenyl)-3-(heptanimidoyl)-2-thiourea hydrochloride there is obtained 1-(4-aminophenyl)-3-(heptanimidoyl)-2-thiourea.
Sources & evidence
- ORD record
- ord-b8037bdcff0a460d9670ca8f140d3b85
- Source dataset
- uspto-grants-1976_10
- Patent number
- US03984467
Reaction notes
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