Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | HCID 54246480 | HCID 54246480 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Iaa-94 | HCID 3667 | — |
Reaction Steps
A solution of tert.-butyl (1-oxo-2-cyclopentyl-2-methyl-6,7-dichloro-5-indanyloxy)acetate (4.13 g., 0.01 mole) and p-toluenesulfonic acid (0.3 g.) in benzene (50 ml.) is refluxed for ten minutes then cooled to 25°C. affording (1-oxo-2-cyclopentyl-2-methyl-6,7-dichloro-5-indanyloxy)acetic acid which melts at 113°-114°C. after recrystallization from acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US03984465 |
|---|
| Source dataset | uspto-grants-1976_10 |
|---|
| ORD ID | ord-84ba811d246849109557cd1c31cfd61f |
|---|
| Source note | uspto-grants-1976_10 |
|---|
