化工社化工社 化学情報印刷レポート · 研究参考用
2,3-Dichloroanisole → 2',3'-Dichloro-4'-methoxy-2-methylbutyrophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3-Dichloroanisole | HCID 16126 | — |
| 反応物 | Butanoyl chloride, 2-methyl- | HCID 93697 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 2',3'-Dichloro-4'-methoxy-2-methylbutyrophenone | HCID 20358455 | — |
反応手順
By following the procedure described in Example 5, Step A, using as the reactants 2,3-dichloroanisole (100 g., 0.565 mole), 2-methylbutyryl chloride (.75 g., 0.62 mole), aluminum chloride (84 g., 0.62 mole) and methylene chloride (400 ml.), there is obtained 2',3'-dichloro-4'-methoxy-2-methylbutyrophenone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03984465 |
| 出典データセット | uspto-grants-1976_10 |
| ORD ID | ord-f231e2f7ba9d48729951e8d55a73bbc5 |
| 出典メモ | uspto-grants-1976_10 |