HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 2,2,3-Trimethyl-5-methoxy-6,7-dichloro-1-indanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2,3-Dimethyl-5-methoxy-6,7-dichloro-1-indanone | HCID 20358441 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | 2,2,3-Trimethyl-5-methoxy-6,7-dichloro-1-indanone | HCID 20358451 | — |
Reaction Steps
By following the procedure described in Example 5, Step E, using as the reactants 2,3-dimethyl-5-methoxy-6,7-dichloro-1-indanone (13 g., 0.05 mole), sodium hydride (1.44 g., 0.06 mole), 1,2-dimethoxyethane (500 ml.) and methyl iodide (8 ml.), there is obtained 2,2,3-trimethyl-5-methoxy-6,7-dichloro-1-indanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984465 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-15555febb1fa44138a2448732d437678 |
| Source note | uspto-grants-1976_10 |