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HRID 1287463作成日：2026年10月25日

2,3-Dichlorothioanisole → 2',3'-Dichloro-4'-methylthio-2-cyclopentylacetophenone

https://huagongshe.com/reaction/1287463

反応式

関与物質

役割名称HCID仕込み量
反応物2,3-DichlorothioanisoleHCID 2758224—
反応物Cyclopentylacetyl chlorideHCID 3485182—
反応物Aluminum(III) ChlorideHCID 6451240—
溶媒DichloromethaneHCID 6344—
生成物2',3'-Dichloro-4'-methylthio-2-cyclopentylacetophenoneHCID 20358446—

反応手順

2',3'-Dichloro-4'-methylthio-2-cyclopentylacetophenone is prepared following substantially the same procedure described in Example 10, Step A, using the following substances: 2,3-dichlorothioanisole (63.1 g., 0.327 mole), methylene chloride (300 ml.), cyclopentylacetyl chloride (52.7 g., 0.367 mole) and aluminum chloride (48.0 g., 0.36 mole).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US03984465
出典データセットuspto-grants-1976_10
ORD IDord-05036d1afd634429b19f1fb07a66b6fc
出典メモuspto-grants-1976_10