HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 2-Cyclopentyl-2-methyl-5-methylthio-6,7-dichloro-1-indanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-Cyclopentyl-5-methylthio-6,7-dichloro-1-indanone | HCID 20358454 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | 2-Cyclopentyl-2-methyl-5-methylthio-6,7-dichloro-1-indanone | HCID 20358461 | — |
Reaction Steps
2-Cyclopentyl-2-methyl-5-methylthio-6,7-dichloro-1-indanone is prepared following substantially the same procedure described in Example 10, Step D, using the following substances: 2-cyclopentyl-5-methylthio-6,7-dichloro-1-indanone (7.9 g., 0.025 mole), 1,2-dimethoxyethane (200 ml.), sodium hydride (660 mg., 0.0275 mole) and methyl iodide (7.5 ml.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984465 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-cb3b46671ef747368ffd0e4c00b0461f |
| Source note | uspto-grants-1976_10 |