HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → (1-Oxo-2-cyclopentyl-2-methyl-6,7-dichloro-5-indanylthio)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 13827615 | HCID 13827615 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | (1-Oxo-2-cyclopentyl-2-methyl-6,7-dichloro-5-indanylthio)acetic acid | HCID 20358448 | — |
Reaction Steps
(1-Oxo-2-cyclopentyl-2-methyl-6,7-dichloro-5-indanylthio)acetic acid is prepared following substantially the same procedure described in Example 10, Step F, using the following substances: 2-cyclopentyl-2-methyl-5-mercapto-6,7-dichloro-1-indanone (3.47 g., 0.01 mole), DMF (40 ml.), potassium carbonate (2.78 g., 0.02 mole) and ethyl bromoacetate (2.9 g., 0.02 mole).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03984465 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-e39873d148b74e6bbde3d84d7c96cd2a |
| Source note | uspto-grants-1976_10 |