Phenyl isocyanate → HCID 12500226, compound
Reaction equation
[NH2:1][C:2]1[NH:3][C:4]2[C:9]([C:10]=1[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=[CH:8][CH:7]=[CH:6][CH:5]=2.[C:17]1([N:23]=[C:24]=[O:25])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[C:11]1([C:10]2[C:9]3[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=3)[NH:3][C:2]=2[NH:1][C:24]([NH:23][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[O:25])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1Participants
3
Procedure
The compound is obtained according to Example 34 by reacting 2-amino-3-phenylindole (m.p. 220°-223° C) with phenylisocyanate. M.p. 210°-212° C.
Workup
- customThe compound is obtained
Sources & evidence
- ORD record
- ord-a919bbf1154f44f48e7336be90e7c0e6
- Source dataset
- uspto-grants-1976_10
- Patent number
- US03984563
Reaction notes
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