HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromophenylhydrazine hydrochloride → 3-Phthalimido-6-bromo-1,2,3,4-tetrahydrocarbazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromophenylhydrazine hydrochloride | HCID 12157 | — |
| Reactant | 2-(4-oxocyclohexyl)-2,3-dihydro-1H-isoindole-1,3-dione | HCID 11998391 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | 3-Phthalimido-6-bromo-1,2,3,4-tetrahydrocarbazole | HCID 18944254 | 104.1% |
Reaction Steps
Reaction of 4-bromophenylhydrazine hydrochloride (4.0 g, 18.1 mmol) with 4-phthalimido-cyclohexanone (4.39 g, 18.1 mmol) in refluxing n-butanol for 20 min, followed by cooling, filtration, and evaporation of the filtrate to dryness yielded 3-phthalimido-6-bromo-1,2,3,4-tetrahydrocarbazole as an orange solid (7.45 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05464864 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-356706dc8cf34c75a7037dfde7dad757 |
| Source note | uspto-grants-1995_11 |