Ethyl chloroacetate → HCID 12797320, compound

HRID 1287668Notes

Reaction equation

HRID 1287668 reaction equation
[F:1][C:2]1[CH:18]=[CH:17][C:5]([O:6][C:7]2[CH:8]=[C:9]([CH:13]([CH3:16])[CH:14]=[O:15])[CH:10]=[CH:11][CH:12]=2)=[CH:4][CH:3]=1.CC[O:21]C(CCl)=O>>[F:1][C:2]1[CH:18]=[CH:17][C:5]([O:6][C:7]2[CH:8]=[C:9]([CH:13]([CH3:16])[C:14]([OH:21])=[O:15])[CH:10]=[CH:11][CH:12]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 7751Ethyl chloroacetateHCID 21506167HCID 21506167, compound

Product 1

HCID 12797320HCID 12797320, compound

Procedure

2-[m-(p-fluorophenoxy)phenyl]propionaldehyde, which has been synthetically prepared in accordance with Example 1 from 3-(p-fluoro-phenoxyphenyl)acetophenone (boiling point: 137° - 138° C./0.5 mmHg) and ethyl ester of chloroacetic acid, is subjected to oxidation in the manner described in Example 1. There is thus obtained the purposed product in a form of oily substance having the melting point of 175° - 176° C./0.5 mmHg.

Workup

  1. customThere is thus obtained the purposed product in a form of oily substance

Sources & evidence

ORD record
ord-7ebe93bca60c4c30bc20f02e8a8096a0
Source dataset
uspto-grants-1976_10
Patent number
US03985779

Reaction notes

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