HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 20377231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Trichloro(2-chloroethyl)silane | HCID 80386 | — |
| Product | HCID 20377231 | HCID 20377231 | 80.5% |
Reaction Steps
An amount of 40.8 g of 2-chloroethyl-trichlorosilane is dissolved in 71.5 g of acetic acid anhydride, and the solution allowed to stand at room temperature for 21 hours in a closed vessel. The reaction product is concentrated in vacuo to obtain 44.6 g of 2-chloro-ethyl-tris-(acetyloxy)-silane, B.P.: 85° - 88° /0.1 Torr, nD20 = 1.6687.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03985780 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-f36c1de8cde7409d882941b64f49d6ff |
| Source note | uspto-grants-1976_10 |