HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 21506104, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | 3-Amino-5-methylsulphamyl-4-phenoxy-benzoic acid | HCID 21506014 | — |
| Reactant | 5-n-Butylsulphamyl-4-chloro-3-nitro-benzoic acid | HCID 21506016 | — |
| Reactant | 4-Chloro-5-dimethylsulphamyl-3-nitro-benzoic acid | HCID 21506054 | — |
| Reactant | 3-Amino-5-n-butylsulphamyl-5-phenoxy-benzoic acid | HCID 68140743 | — |
| Product | HCID 21506104 | HCID 21506104 | — |
Reaction Steps
The starting materials, 4-chloro-5-dimethylsulphamyl-3-nitro-benzoic acid and 5-n-butylsulphamyl-4-chloro-3-nitro-benzoic acid, were new and were obtained as described for the starting material of Example 2 by substituting aqueous dimethylamine (3.6 g containing 1.5 g of dimethylamine) and n-butylamine (2.2 g), respectively, for the aqueous methylamine, and had melting points of 233-235° C, and 196-198° C, respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03985777 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-9957943bcbd5444f9ec62a4fcb7edd56 |
| Source note | uspto-grants-1976_10 |