HCID 21506056, compound → HCID 21506132, compound

HRID 1287732Notes

Reaction equation

HRID 1287732 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[C:11]([S:22](=[O:25])(=[O:24])[NH2:23])[C:12]=1[NH:13][C:14]1[CH:19]=[CH:18][C:17]([CH3:20])=[CH:16][C:15]=1[CH3:21])[C:7]([OH:9])=[O:8])([O-])=O.N(C1C(S(=O)(=O)N)=CC(C(O)=O)=CC=1[N+]([O-])=O)C1C=CC=CC=1>>[NH2:1][C:4]1[CH:5]=[C:6]([CH:10]=[C:11]([S:22](=[O:25])(=[O:24])[NH2:23])[C:12]=1[NH:13][C:14]1[CH:19]=[CH:18][C:17]([CH3:20])=[CH:16][C:15]=1[CH3:21])[C:7]([OH:9])=[O:8]

Participants

3

Reactant 2

HCID 21506056HCID 21506056, compoundHCID 215060714-Anilino-3-nitro-5-sulphamyl-benzoic acid

Product 1

HCID 21506132HCID 21506132, compound

Procedure

By substituting 3-nitro-5-sulphamyl-4-(2,4-dimethylanilino)-benzoic acid for the 4-anilino-3-nitro-5-sulphamyl-benzoic acid of Example 9 B, the above compound was obtained with a melting point of 241°-241.5° C after recrystallization from ethanol.

Workup

  1. customthe above compound was obtained with a melting point of 241°-241.5° C
  2. customafter recrystallization from ethanol

Sources & evidence

ORD record
ord-c2587ab70ece41c6a49eaf5f4897f509
Source dataset
uspto-grants-1976_10
Patent number
US03985777

Reaction notes

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