4-Anilino-3-nitro-5-sulphamyl-benzoic acid → HCID 21506115, compound

HRID 1287746Notes

Reaction equation

HRID 1287746 reaction equation
[O:1]1[CH2:6][CH2:5][N:4]([C:7]2[C:15]([S:16](=[O:19])(=[O:18])[NH2:17])=[CH:14][C:10]([C:11]([OH:13])=[O:12])=[CH:9][C:8]=2[N+:20]([O-])=O)[CH2:3][CH2:2]1.N(C1C(S(=O)(=O)N)=CC(C(O)=O)=CC=1[N+]([O-])=O)C1C=CC=CC=1>>[NH2:20][C:8]1[CH:9]=[C:10]([CH:14]=[C:15]([S:16](=[O:18])(=[O:19])[NH2:17])[C:7]=1[N:4]1[CH2:3][CH2:2][O:1][CH2:6][CH2:5]1)[C:11]([OH:13])=[O:12]

Participants

3

Reactant 2

HCID 215060714-Anilino-3-nitro-5-sulphamyl-benzoic acidHCID 21506129HCID 21506129, compound

Product 1

HCID 21506115HCID 21506115, compound

Procedure

By substituting 4-morpholino-3-nitro-5-sulphamyl-benzoic acid for the 4-anilino-3-nitro-5sulphamyl-benzoic acid of Example 9 B, the above compound was obtained with a melting point of 297° C (decomp.) after recrystallization from aqueous methanol.

Workup

  1. customthe above compound was obtained with a melting point of 297° C (decomp.)
  2. customafter recrystallization from aqueous methanol

Sources & evidence

ORD record
ord-d7b8a65581a844b4bf493b0b3ca5dd47
Source dataset
uspto-grants-1976_10
Patent number
US03985777

Reaction notes

Loading…