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HRID1287763

反应详情

EQUATION

反应方程式

HRID 1287763 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：NS(=O)(=O)c1cc(C(=O)O)cc([N+](=O)[O-])c1Oc1ccccc1
HCID119926

3-Nitro-4-phenoxy-5-sulfamoylbenzoic acid

C13H10N2O7S

PRODUCTS

生成物

1
结构：NS(=O)(=O)c1cc(C(=O)Cl)cc([N+](=O)[O-])c1Oc1ccccc1
HCID21506035

3-Nitro-4-phenoxy-5-sulfamoylbenzoyl chloride

C13H9ClN2O6S

PROCEDURE

实验过程

A mixture of 3-nitro-4-phenoxy-5-sulphamyl-benzoic acid (5 g) and thionyl chloride (50 ml) was heated on a steam bath for 5 hours. After evaporation in vacuo to dryness, the compound was obtained as a crude product, which was used in the next step without further purification.

WORKUP

后处理

  1. temperaturewas heated on a steam bath for 5 hours
  2. customAfter evaporation in vacuo to dryness