HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 85774566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 1-Bromohexane | HCID 8101 | — |
| Reactant | 3-Amino-4-phenoxy-5-sulfamoylbenzoic acid | HCID 119927 | — |
| Solvent | 1-Hexanol | HCID 8103 | — |
| Product | HCID 85774566 | HCID 85774566 | — |
Reaction Steps
A mixture of 3-amino-4-phenoxy-5-sulphamyl-benzoic acid (4.62 g), 1-bromo-n-hexane (5 g), methanesulphonic acid (0.05 ml), and n-hexanol (40 ml) was refluxed for 60 hours. After cooling, the precipitated n-hexyl-3-n-hexylamino-4-phenoxy-5-sulphamyl-benzoate was collected and recrystallized from hexanol. The melting point was 137°-138° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03985777 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-18e2ccc5fc4b4b69b3ea0ef6d6badb96 |
| Source note | uspto-grants-1976_10 |