HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 21506073, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 3-Amino-4-phenoxy-5-sulfamoylbenzoic acid | HCID 119927 | — |
| Product | HCID 21506073 | HCID 21506073 | — |
Reaction Steps
A mixture of 3-amino-4-phenoxy-5-sulphamyl-benzoic acid (3.08 g), allyl bromide (7.25 g), and dry ethanol was refluxed for 24 hours. After cooling, the precipitated ethyl-3-allylamino-4-phenoxy-5-sulphamyl-benzoate was filtered off and recrystallized from ethanol. The melting point of the ester was 153°-154° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03985777 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-586019f437fe4f64830b095696f9055f |
| Source note | uspto-grants-1976_10 |