HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-benzylamino-5-dimethylsulphamyl-4-phenoxy-benzoate → 3-Benzylamino-5-(n-butylsulphamyl)-4-phenoxy-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-benzylamino-5-dimethylsulphamyl-4-phenoxy-benzoate | HCID 21506051 | — |
| Reactant | HCID 21506077 | HCID 21506077 | — |
| Product | 3-Benzylamino-5-(n-butylsulphamyl)-4-phenoxy-benzoic acid | HCID 21506097 | — |
Reaction Steps
By substituting in step B above ethyl 3-benzylamino-5-(n-butylsulphamyl)- 4-phenoxy-benzoate for the ethyl 3-benzylamino-5-dimethylsulphamyl-4-phenoxy-benzoate, and after recrystallization from ethanol, the above compound was obtained with a melting point of 212° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03985777 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-e55a0e4c3abe4c789a4cbe049f4497e4 |
| Source note | uspto-grants-1976_10 |