HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 12308266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | beta-Aminobeta-ethoxyacrylic acid ethyl ester | HCID 278451 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 12308266 | HCID 12308266 | 64% |
Reaction Steps
Upon boiling a solution of 5.3 g of benzaldehyde and 15.9 g of 3-amino-3-ethoxyacrylic acid ethyl ester in 30 ml of alcohol for 12 hours, 2-amino-4-phenyl-6-ethoxy-4,5-dihydropyridine-3,5-dicarboxylic acid diethyl ester of melting point 119° C (isopropanol) is obtained. Yield: 64% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03985886 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-a5c16429301940fb95e37f95f58b94dc |
| Source note | uspto-grants-1976_10 |