HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylazepan-4-one → 4-[2-(4,4-Dimethyl-2-oxazolin-2-yl)phenyl]-2,3,4,5,6,7-hexahydro-4-hydroxy-1-methylazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylazepan-4-one | HCID 262586 | — |
| Reactant | 2-(2-Bromophenyl)-4,4-dimethyl-4,5-dihydro-1,3-oxazole | HCID 289296 | — |
| Product | 4-[2-(4,4-Dimethyl-2-oxazolin-2-yl)phenyl]-2,3,4,5,6,7-hexahydro-4-hydroxy-1-methylazepine | HCID 21506815 | — |
Reaction Steps
Reaction of 2,3,4,5,6,7-hexahydro-1-methylazepin-4-one and 2-(2-bromophenyl)-4,4-dimethyl-2-oxazoline by the method described in Example 1c provides 4-[2-(4,4-dimethyl-2-oxazolin-2-yl)phenyl]-2,3,4,5,6,7-hexahydro-4-hydroxy-1-methylazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03985889 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-874686ac25474b30895ea07e188cbf55 |
| Source note | uspto-grants-1976_10 |