HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 53703656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 20315068 | HCID 20315068 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53703656 | HCID 53703656 | — |
Reaction Steps
209.5 parts of 2-(2-chloro-2-cyanoethyl) benzoic acid are made into a paste in 220 parts of toluene and 125 parts of thionyl chloride and the mixture is refluxed until the acid completely dissolves. Then the surplus thionyl chloride and toluene are eliminated under reduced pressure. 2-(2-chloro-2-cyanoethyl) benzoyl chloride is obtained which is liquid at normal temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987027 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-dee2319d3f1e4258ac68415d971a4e93 |
| Source note | uspto-grants-1976_10 |