HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 53717999, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 3041687 | HCID 3041687 | — |
| Product | HCID 53717999 | HCID 53717999 | — |
Reaction Steps
17.3 parts of 4-(2-cyanovinyl) benzoic acid are made into a paste in 80 parts of thionyl chloride and the mixture is refluxed for 15 minutes. Then the surplus thionyl chloride is eliminated under reduced pressure and the 4-(2-cyanovinyl) benzoyl chloride, which is thus obtained, is purified by being recrystallized in xylene. M.P.: 154° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987027 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-3e3b837ae0de407fb8574c9324d37c0f |
| Source note | uspto-grants-1976_10 |