Ethyl chloroformate → HCID 68140457, compound

HRID 1288118Notes

Reaction equation

HRID 1288118 reaction equation
[CH2:1]1[C:15]2[C:6](=[N:7][C:8]3[CH:9]=[CH:10][CH:11]=[CH:12][C:13]=3[CH:14]=2)[CH2:5][CH2:4][NH:3][CH2:2]1.[Cl:16][C:17]([O:19][CH2:20][CH3:21])=[O:18]>>[ClH:16].[CH2:20]([O:19][C:17]([N:3]1[CH2:2][CH2:1][C:15]2[C:6](=[N:7][C:8]3[CH:9]=[CH:10][CH:11]=[CH:12][C:13]=3[CH:14]=2)[CH2:5][CH2:4]1)=[O:18])[CH3:21]

Participants

3

Reactant 2

HCID 10928Ethyl chloroformateHCID 21503403HCID 21503403, compound

Product 1

HCID 68140457HCID 68140457, compoundYield 64%

Procedure

1,2,4,5-Tetrahydro-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester hydrochloride was prepared from 1,2,4,5-tetrahydro-3H-azepino[4,5-b]quinoline and ethyl chloroformate analogous to Example 63.

Sources & evidence

ORD record
ord-f0e8230f437e4b2aa0692225c10697b3
Source dataset
uspto-grants-1976_10
Patent number
US03987047

Reaction notes

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