Ethyl chloroformate → HCID 53729716, compound

HRID 1288122Notes

Reaction equation

HRID 1288122 reaction equation
[Cl:1][C:2]1[C:11]2[N:10]=[C:9]3[CH2:12][CH2:13][NH:14][CH2:15][CH2:16][C:8]3=[C:7]([CH3:17])[C:6]=2[CH:5]=[CH:4][CH:3]=1.Cl[C:19]([O:21][CH2:22][CH3:23])=[O:20]>>[CH2:22]([O:21][C:19]([N:14]1[CH2:15][CH2:16][C:8]2[C:9](=[N:10][C:11]3[C:2]([Cl:1])=[CH:3][CH:4]=[CH:5][C:6]=3[C:7]=2[CH3:17])[CH2:12][CH2:13]1)=[O:20])[CH3:23]

Participants

3

Reactant 2

HCID 10928Ethyl chloroformateHCID 21503522HCID 21503522, compound

Product 1

HCID 53729716HCID 53729716, compoundYield 70%

Procedure

7-Chloro-1,2,4,5-tetrahydro-11-methyl-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester was prepared from 7-chloro-1,2,4,5-tetrahydro-11methyl-3H-azepino[4,5-b]quinoline and ethyl chloroformate analogous to Example 63.

Sources & evidence

ORD record
ord-870f5103816b4eb4a2abf89c54999b16
Source dataset
uspto-grants-1976_10
Patent number
US03987047

Reaction notes

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